Advanced Materials Synthesis Glovebox with Integrated Heated Rectangular Chamber and Water Chiller
The system integrates a dry,oxygen-free atmosphere,controlled high-temperature reactions and rapid cooling/quenching. The main box provides an inert environment typically below1ppm moisture/oxygen. A through-wall heated square chamber supports synthesis,annealing and sintering; an integrated chiller/cooling stage quenches hot samples to preserve phases/microstructures. This closed synthesis-to-treatment/packaging platform expands inert-atmosphere materials research. A tilted removable8mm tempered safety-glass window uses a3/8-inch OMEGA seal. Two adjustable shelf levels and a mobile steel stand950mm high including swivel casters are provided. The large304 stainless square airlock has a lifting door and measures400mm×400mm×600mm; the small airlock is150mm diameter x300mm long with manual evacuation/refill. The large chamber has movable/extending stainless trays:three removable levels with flat-plate heating,PID control at150℃,independent temperature display,error±1℃,accuracy0.1℃ and an external insulation cover. Timed touchscreen automatic purging handles gas changes and accidental moisture/oxygen entry; wire-reinforced plastic KF25 tubing and a KF25 hose barb connect the purge system. Oxygen analyzer: imported US Avcray (electrochemical), not domestically manufactured/assembled, with third-party data assurance; other oxygen analyzer: GE oxy.IQ™ Oxygen Transmitter. Moisture analyzer: imported UK MICHELL, selected for the operating environment, not domestically manufactured/assembled, with third-party data assurance; other moisture analyzer: GE VeriDri™ Dew-Point Transmitter. Pump start/stop timing is included. An imported UK Edwards RV12 provides12m³/h and ultimate vacuum2x10⁻³mbar,with independent airlock evacuation/control. Listed certifications: ISO9001, CE and UL. One-year warranty and lifetime repair. Consult the manual's danger, warning and caution provisions.
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Overview
Specifications
| Parameter | Value |
|---|---|
| Boxes - Dimensions | 1200mm×920mm×800mm |
| Box - Structure | Total stainless steel structure (Type 304) |
| Box - thickness | 3 mm |
| Box - Volume | 2.3 m³ |
| Box - Front Window - Glass thickness | 8 mm |
| Boxes - Front Window - Seal Circle | 3/8 inches thick OMEGA seal. |
| Boxes - Gloves | 8 in |
| Boxes - Gloves - Materials | Hard aluminium alloy gloves (combustion resistant, aluminum anode oxide) |
| Boxes - Gloves Ports - caliber | 220 mm |
| Boxes - Gloves - Materials | Original butyl rubber imports, United States |
| Box - Glove - Thickness | 0.4 mm |
| Box - Filter - Aperture | 0.3 μm |
| Boxes - Lighting | The box is equipped with a reaction-proof light-saving light, soft light. |
| Boxes - leakage rate | <0.001 vol%/h |
| Boxes - shelf | Two-tier adjustable shelving |
| Box-pore-pore power circuit boards-power | 220V±10% 50Hz±10% |
| Boxes - Interfaces | Multiple standard KF-40 interfaces set |
| Boxes - stand-ups - materials | Steel |
| Boxes - strench - high-bearing wheel | 950 mm |
| Boxes - strangling - ankles | A thousand-way wheel. |
| Transition class -- large transition class -- structure | Square |
| Transition class -- large transition class -- materials | 304 stainless steel. |
| Transition class -- large transition class -- door | ♪ Up the door ♪ |
| Transition class -- large transition class -- size | 400mm×400mm×600mm |
| Transition class -- large transition module -- vacuum [Large, small right overboard requires a vacuum belt to be displayed] | <1 bar |
| Transition class -- small transition module -- materials | stainless steel type 304 (1.4301) |
| Transition class - small transition module - thickness | 2 mm |
| Transition class -- small transition class -- diameter | 150 mm |
| Transition class -- small transit class -- long | 300 mm |
| Transition class -- small transition module -- vacuum [Large, small right overboard requires a vacuum belt to be displayed] | <1 bar |
| Transition module - Large Transition module - Tray - Materials [Large over-class configuration] | stainless steel. |
| Transition class -- large transition module -- pallet -- move [Large over-class configuration] | Free to move extension |
| Transition class -- large transition module -- tray -- layers [Large over-class configuration] | 3 层 |
| Transition class -- large transition module -- palletization -- disassembly [Large over-class configuration] | Dismantling |
| Transition class -- large transition module -- heating -- layers [Large over-class configuration] | 3 层 |
| Transition class - Large Transition class - Heating - Method [Large over-class configuration] | Heating tablets |
| Transition module - Large Transition module - Heating - Temperature Control [Large over-class configuration] | PID Smart Temperature Control |
| Transition class - Large Transition class - Heating - Temperature [Large over-class configuration] | 150 ℃ |
| Transition class - Large transition module - Heating - Temperature display [Large over-class configuration] | Transition module temperature independent. |
| Transition class -- large transition module -- heating -- error [Large over-class configuration] | ±1 ℃ |
| Transition class - Large Transition class - Heating - Precision [Large over-class configuration] | 0.1 ℃ |
| Transition class - Large Transition class - Heating - Temperature [Large over-class configuration] | The outside inverted. |
| Purge system - valve to box pipe integration | KF25 has a strong connection to the steel silk-sweet tube. |
| Cleaning system -- external interface | KF25 tower. |
| Analyzers - oxygen analysers - dimensions | 205 mm（L） x 80 mm（W） x 60 mm（H） |
| Analyzers - oxygen analysers - range measurement | 0-1000 Ppm |
| Analyzer-water analyser-size | 205 mm（L） x 80 mm（W） x 60 mm（H） |
| Analyzers - hydrometric analysers - range of measurements | 0-1000 ppm |
| Vacuum system - Vacuum pump - Model | RV12 |
| Vacuum systems - vacuum pumps - flow | 12 m³/h |
| Vacuum systems - Vacuum pumps - limit vacuum | 2x10⁻³mbar |
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